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Machine-Assisted Organic Synthesis.

Ley SV, Fitzpatrick DE, Myers RM, Battilocchio C, Ingham RJ - Angew. Chem. Int. Ed. Engl. (2015)

Bottom Line: In this Review we describe how the advent of machines is impacting on organic synthesis programs, with particular emphasis on the practical issues associated with the design of chemical reactors.Additional technologies have been developed to facilitate more specialized reaction techniques such as electrochemical and photochemical methods.All of these areas create both opportunities and challenges during adoption as enabling technologies.

View Article: PubMed Central - PubMed

Affiliation: Department of Chemistry, University of Cambridge, Lensfield Road, Cambridge, CB2 1EW (UK). svl1000@cam.ac.uk.

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An inductive system used for the machine‐assisted heating of a continuous‐flow reactor column. Reprinted from Ref. 54a.
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fig11: An inductive system used for the machine‐assisted heating of a continuous‐flow reactor column. Reprinted from Ref. 54a.

Mentions: An alternative to microwave methods is inductive heating, which is an effective method for heating reactions to high temperatures. Kirschning and co‐workers have reported the use of superparamagnetic nanoparticles coated with silica gel and steel beads as efficient materials to use in a fix‐bed flow reactor to rapidly achieve high temperatures under exposure to an inductive magnetic field (Figure 11).53


Machine-Assisted Organic Synthesis.

Ley SV, Fitzpatrick DE, Myers RM, Battilocchio C, Ingham RJ - Angew. Chem. Int. Ed. Engl. (2015)

An inductive system used for the machine‐assisted heating of a continuous‐flow reactor column. Reprinted from Ref. 54a.
© Copyright Policy - open-access
Related In: Results  -  Collection

Show All Figures
getmorefigures.php?uid=PMC4834626&req=5

fig11: An inductive system used for the machine‐assisted heating of a continuous‐flow reactor column. Reprinted from Ref. 54a.
Mentions: An alternative to microwave methods is inductive heating, which is an effective method for heating reactions to high temperatures. Kirschning and co‐workers have reported the use of superparamagnetic nanoparticles coated with silica gel and steel beads as efficient materials to use in a fix‐bed flow reactor to rapidly achieve high temperatures under exposure to an inductive magnetic field (Figure 11).53

Bottom Line: In this Review we describe how the advent of machines is impacting on organic synthesis programs, with particular emphasis on the practical issues associated with the design of chemical reactors.Additional technologies have been developed to facilitate more specialized reaction techniques such as electrochemical and photochemical methods.All of these areas create both opportunities and challenges during adoption as enabling technologies.

View Article: PubMed Central - PubMed

Affiliation: Department of Chemistry, University of Cambridge, Lensfield Road, Cambridge, CB2 1EW (UK). svl1000@cam.ac.uk.

Show MeSH
Related in: MedlinePlus