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Crystal structure of the adduct (4-chloro-phen-yl)(4-hy-droxy-piperidin-1-yl)methanone-(4-chloro-phen-yl)(piperidin-1-yl)methanone (0.75/0.25).

Revathi BK, Reuben Jonathan D, Kalai Sevi K, Dhanalakshmi K, Usha G - Acta Crystallogr E Crystallogr Commun (2015)

Bottom Line: In the title compound, 0.75C12H14ClNO2·0.25C12H14ClNO, which is an adduct comprising 0.75 4-hy-droxy-piperidin-1-yl or 0.25 4-piperidin-1-yl substituents on a common (4-chloro-phen-yl)methanone component; the dihedral angles between the benzene ring and the two piperidine rings are 51.6 (3) and 89.5 (7)°, respectively.The hy-droxy-piperidine ring is in a bis-ectional oriention (bi) with the phenyl ring.In the crystal, inter-molecular O-H⋯O hydrogen bonds between the hy-droxy-piperidine group and the keto O atom lead to the formation of chains extending along the c- axis direction.

View Article: PubMed Central - HTML - PubMed

Affiliation: PG and Research Department of Physics, Queen Mary's College, Chennai-4, Tamilnadu, India.

ABSTRACT
In the title compound, 0.75C12H14ClNO2·0.25C12H14ClNO, which is an adduct comprising 0.75 4-hy-droxy-piperidin-1-yl or 0.25 4-piperidin-1-yl substituents on a common (4-chloro-phen-yl)methanone component; the dihedral angles between the benzene ring and the two piperidine rings are 51.6 (3) and 89.5 (7)°, respectively. The hy-droxy-piperidine ring is in a bis-ectional oriention (bi) with the phenyl ring. In the crystal, inter-molecular O-H⋯O hydrogen bonds between the hy-droxy-piperidine group and the keto O atom lead to the formation of chains extending along the c- axis direction.

No MeSH data available.


Related in: MedlinePlus

The molecular structure of the major (73%) 4-hydroxypiperidin-1-yl substituted component of the title adduct, showing atom numbering, with displacement ellipsoids drawn at the 30% probability level.
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Fap1: The molecular structure of the major (73%) 4-hydroxypiperidin-1-yl substituted component of the title adduct, showing atom numbering, with displacement ellipsoids drawn at the 30% probability level.


Crystal structure of the adduct (4-chloro-phen-yl)(4-hy-droxy-piperidin-1-yl)methanone-(4-chloro-phen-yl)(piperidin-1-yl)methanone (0.75/0.25).

Revathi BK, Reuben Jonathan D, Kalai Sevi K, Dhanalakshmi K, Usha G - Acta Crystallogr E Crystallogr Commun (2015)

The molecular structure of the major (73%) 4-hydroxypiperidin-1-yl substituted component of the title adduct, showing atom numbering, with displacement ellipsoids drawn at the 30% probability level.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC4645011&req=5

Fap1: The molecular structure of the major (73%) 4-hydroxypiperidin-1-yl substituted component of the title adduct, showing atom numbering, with displacement ellipsoids drawn at the 30% probability level.
Bottom Line: In the title compound, 0.75C12H14ClNO2·0.25C12H14ClNO, which is an adduct comprising 0.75 4-hy-droxy-piperidin-1-yl or 0.25 4-piperidin-1-yl substituents on a common (4-chloro-phen-yl)methanone component; the dihedral angles between the benzene ring and the two piperidine rings are 51.6 (3) and 89.5 (7)°, respectively.The hy-droxy-piperidine ring is in a bis-ectional oriention (bi) with the phenyl ring.In the crystal, inter-molecular O-H⋯O hydrogen bonds between the hy-droxy-piperidine group and the keto O atom lead to the formation of chains extending along the c- axis direction.

View Article: PubMed Central - HTML - PubMed

Affiliation: PG and Research Department of Physics, Queen Mary's College, Chennai-4, Tamilnadu, India.

ABSTRACT
In the title compound, 0.75C12H14ClNO2·0.25C12H14ClNO, which is an adduct comprising 0.75 4-hy-droxy-piperidin-1-yl or 0.25 4-piperidin-1-yl substituents on a common (4-chloro-phen-yl)methanone component; the dihedral angles between the benzene ring and the two piperidine rings are 51.6 (3) and 89.5 (7)°, respectively. The hy-droxy-piperidine ring is in a bis-ectional oriention (bi) with the phenyl ring. In the crystal, inter-molecular O-H⋯O hydrogen bonds between the hy-droxy-piperidine group and the keto O atom lead to the formation of chains extending along the c- axis direction.

No MeSH data available.


Related in: MedlinePlus