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Shynthesis and Characterizations of Calcium Hydroxyapatite Derived from Crabs Shells (Portunus pelagicus) and Its Potency in Safeguard against to Dental Demineralizations.

Raya I, Mayasari E, Yahya A, Syahrul M, Latunra AI - Int J Biomater (2015)

Bottom Line: Calcination was conducted to crab's shells of Portunus pelagicus at temperature of 1000°C for 5 hours.The results of calcination was reacted with (NH4)2HPO4, then dried at 110°C for 5 hours.The results showed that the rate of tooth demineralization in acetate buffer decreased significantly with the provision of hydroxyapatite into a solution where the addition of the magnitude of hydroxyapatite is greater decrease in the rate of tooth demineralization.

View Article: PubMed Central - PubMed

Affiliation: Chemistry Department, Faculty of Mathematics and Natural Sciences, Hasanuddin University, Makassar 90245, Indonesia.

ABSTRACT
Crab's shells of Portunus pelagicus species were used as raw materials for synthesis of hydroxyapatite were used for protection against demineralization of teeth. Calcination was conducted to crab's shells of Portunus pelagicus at temperature of 1000°C for 5 hours. The results of calcination was reacted with (NH4)2HPO4, then dried at 110°C for 5 hours. Sintering was conducted to results of precipitated dried with temperature variations 400-1000°C for a hour each variation of temperature then characterized by X-ray diffractometer and FTIR in order to obtain the optimum formation temperature of hydroxyapatite is 800°C. The hydroxyapatite is then tested its effectiveness in protection against tooth demineralization using acetate buffer pH 5.0 with 1 M acetic acid concentration with the addition of hydroxyapatite and time variation of immersion. The results showed that the rate of tooth demineralization in acetate buffer decreased significantly with the provision of hydroxyapatite into a solution where the addition of the magnitude of hydroxyapatite is greater decrease in the rate of tooth demineralization.

No MeSH data available.


Related in: MedlinePlus

The EDXA spectrum of hydroxyapatite (HA) synthesis from crab shells.
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Related In: Results  -  Collection


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fig10: The EDXA spectrum of hydroxyapatite (HA) synthesis from crab shells.

Mentions: While in Figure 10 the EDXA spectrum shows the composition of the synthesis yield was dominated by oxygen (O) up to 59.52%, calcium (Ca) up to 23.76%, and phosphorus (P) up to 13.32%. The composition confirmed the composition of hydroxyapatite. It can be concluded that the synthesis results can be achieved to target.


Shynthesis and Characterizations of Calcium Hydroxyapatite Derived from Crabs Shells (Portunus pelagicus) and Its Potency in Safeguard against to Dental Demineralizations.

Raya I, Mayasari E, Yahya A, Syahrul M, Latunra AI - Int J Biomater (2015)

The EDXA spectrum of hydroxyapatite (HA) synthesis from crab shells.
© Copyright Policy - open-access
Related In: Results  -  Collection

Show All Figures
getmorefigures.php?uid=PMC4508471&req=5

fig10: The EDXA spectrum of hydroxyapatite (HA) synthesis from crab shells.
Mentions: While in Figure 10 the EDXA spectrum shows the composition of the synthesis yield was dominated by oxygen (O) up to 59.52%, calcium (Ca) up to 23.76%, and phosphorus (P) up to 13.32%. The composition confirmed the composition of hydroxyapatite. It can be concluded that the synthesis results can be achieved to target.

Bottom Line: Calcination was conducted to crab's shells of Portunus pelagicus at temperature of 1000°C for 5 hours.The results of calcination was reacted with (NH4)2HPO4, then dried at 110°C for 5 hours.The results showed that the rate of tooth demineralization in acetate buffer decreased significantly with the provision of hydroxyapatite into a solution where the addition of the magnitude of hydroxyapatite is greater decrease in the rate of tooth demineralization.

View Article: PubMed Central - PubMed

Affiliation: Chemistry Department, Faculty of Mathematics and Natural Sciences, Hasanuddin University, Makassar 90245, Indonesia.

ABSTRACT
Crab's shells of Portunus pelagicus species were used as raw materials for synthesis of hydroxyapatite were used for protection against demineralization of teeth. Calcination was conducted to crab's shells of Portunus pelagicus at temperature of 1000°C for 5 hours. The results of calcination was reacted with (NH4)2HPO4, then dried at 110°C for 5 hours. Sintering was conducted to results of precipitated dried with temperature variations 400-1000°C for a hour each variation of temperature then characterized by X-ray diffractometer and FTIR in order to obtain the optimum formation temperature of hydroxyapatite is 800°C. The hydroxyapatite is then tested its effectiveness in protection against tooth demineralization using acetate buffer pH 5.0 with 1 M acetic acid concentration with the addition of hydroxyapatite and time variation of immersion. The results showed that the rate of tooth demineralization in acetate buffer decreased significantly with the provision of hydroxyapatite into a solution where the addition of the magnitude of hydroxyapatite is greater decrease in the rate of tooth demineralization.

No MeSH data available.


Related in: MedlinePlus