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Analysis of Ergot Alkaloids.

Crews C - Toxins (Basel) (2015)

Bottom Line: The principles and application of established and newer methods for the quantitative and semi-quantitative determination of ergot alkaloids in food, feed, plant materials and animal tissues are reviewed.The techniques of sampling, extraction, clean-up, detection, quantification and validation are described.The major procedures for ergot alkaloid analysis comprise liquid chromatography with tandem mass spectrometry (LC-MS/MS) and liquid chromatography with fluorescence detection (LC-FLD).

View Article: PubMed Central - PubMed

Affiliation: Fera Science Ltd., Sand Hutton, North Yorks YO41 1LZ, UK. colin.crews@fera.co.uk.

ABSTRACT
The principles and application of established and newer methods for the quantitative and semi-quantitative determination of ergot alkaloids in food, feed, plant materials and animal tissues are reviewed. The techniques of sampling, extraction, clean-up, detection, quantification and validation are described. The major procedures for ergot alkaloid analysis comprise liquid chromatography with tandem mass spectrometry (LC-MS/MS) and liquid chromatography with fluorescence detection (LC-FLD). Other methods based on immunoassays are under development and variations of these and minor techniques are available for specific purposes.

No MeSH data available.


Related in: MedlinePlus

Structures of representative types of some major ergot alkaloids (EA).
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toxins-07-02024-f001: Structures of representative types of some major ergot alkaloids (EA).

Mentions: Structures of representative types of some major EA are given in Figure 1.


Analysis of Ergot Alkaloids.

Crews C - Toxins (Basel) (2015)

Structures of representative types of some major ergot alkaloids (EA).
© Copyright Policy
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC4488688&req=5

toxins-07-02024-f001: Structures of representative types of some major ergot alkaloids (EA).
Mentions: Structures of representative types of some major EA are given in Figure 1.

Bottom Line: The principles and application of established and newer methods for the quantitative and semi-quantitative determination of ergot alkaloids in food, feed, plant materials and animal tissues are reviewed.The techniques of sampling, extraction, clean-up, detection, quantification and validation are described.The major procedures for ergot alkaloid analysis comprise liquid chromatography with tandem mass spectrometry (LC-MS/MS) and liquid chromatography with fluorescence detection (LC-FLD).

View Article: PubMed Central - PubMed

Affiliation: Fera Science Ltd., Sand Hutton, North Yorks YO41 1LZ, UK. colin.crews@fera.co.uk.

ABSTRACT
The principles and application of established and newer methods for the quantitative and semi-quantitative determination of ergot alkaloids in food, feed, plant materials and animal tissues are reviewed. The techniques of sampling, extraction, clean-up, detection, quantification and validation are described. The major procedures for ergot alkaloid analysis comprise liquid chromatography with tandem mass spectrometry (LC-MS/MS) and liquid chromatography with fluorescence detection (LC-FLD). Other methods based on immunoassays are under development and variations of these and minor techniques are available for specific purposes.

No MeSH data available.


Related in: MedlinePlus