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Crystal structure of 4-[(E)-(4-nitro-benzyl-idene)amino]-phenol.

Atioğlu Z, Akkurt M, Jarrahpour A, Ebrahimi E, Büyükgüngör O - Acta Crystallogr E Crystallogr Commun (2015)

Bottom Line: The asymmetric unit of the title compound, C13H10N2O3, contains four independent mol-ecules (I, II, III and IV).Mol-ecule IV shows whole-mol-ecule disorder over two sets of adjacent sites in a 0.669 (10):0.331 (10) ratio.The layers inter-act by C-H⋯π and weak aromatic π-π stacking inter-actions [centroid-centroid distances = 3.8476 (16), 3.725 (3) and 3.733 (5) Å].

View Article: PubMed Central - HTML - PubMed

Affiliation: İlke Education and Health Foundation, Cappadocia Vocational College, The Medical Imaging Techniques Program, 50420 Mustafapaşa, Ürgüp, Nevşehir, Turkey.

ABSTRACT
The asymmetric unit of the title compound, C13H10N2O3, contains four independent mol-ecules (I, II, III and IV). Mol-ecule IV shows whole-mol-ecule disorder over two sets of adjacent sites in a 0.669 (10):0.331 (10) ratio. The dihedral angles between the aromatic rings are 32.30 (13)° in mol-ecule I, 2.24 (14)° in II, 41.61 (13)° in III, 5.0 (5)° in IV (major component) and 10.2 (3)° in IV (minor component). In the crystal, mol-ecules are linked into layers lying parallel to (024) by C-H⋯O and O-H⋯O inter-actions. The layers inter-act by C-H⋯π and weak aromatic π-π stacking inter-actions [centroid-centroid distances = 3.8476 (16), 3.725 (3) and 3.733 (5) Å].

No MeSH data available.


Related in: MedlinePlus

View of the hydrogen bonding and molecular packing of (I) along a axis. Only H atoms involved in H bonding and atoms of the major disorder component are shown.
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Fap2: View of the hydrogen bonding and molecular packing of (I) along a axis. Only H atoms involved in H bonding and atoms of the major disorder component are shown.


Crystal structure of 4-[(E)-(4-nitro-benzyl-idene)amino]-phenol.

Atioğlu Z, Akkurt M, Jarrahpour A, Ebrahimi E, Büyükgüngör O - Acta Crystallogr E Crystallogr Commun (2015)

View of the hydrogen bonding and molecular packing of (I) along a axis. Only H atoms involved in H bonding and atoms of the major disorder component are shown.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC4384620&req=5

Fap2: View of the hydrogen bonding and molecular packing of (I) along a axis. Only H atoms involved in H bonding and atoms of the major disorder component are shown.
Bottom Line: The asymmetric unit of the title compound, C13H10N2O3, contains four independent mol-ecules (I, II, III and IV).Mol-ecule IV shows whole-mol-ecule disorder over two sets of adjacent sites in a 0.669 (10):0.331 (10) ratio.The layers inter-act by C-H⋯π and weak aromatic π-π stacking inter-actions [centroid-centroid distances = 3.8476 (16), 3.725 (3) and 3.733 (5) Å].

View Article: PubMed Central - HTML - PubMed

Affiliation: İlke Education and Health Foundation, Cappadocia Vocational College, The Medical Imaging Techniques Program, 50420 Mustafapaşa, Ürgüp, Nevşehir, Turkey.

ABSTRACT
The asymmetric unit of the title compound, C13H10N2O3, contains four independent mol-ecules (I, II, III and IV). Mol-ecule IV shows whole-mol-ecule disorder over two sets of adjacent sites in a 0.669 (10):0.331 (10) ratio. The dihedral angles between the aromatic rings are 32.30 (13)° in mol-ecule I, 2.24 (14)° in II, 41.61 (13)° in III, 5.0 (5)° in IV (major component) and 10.2 (3)° in IV (minor component). In the crystal, mol-ecules are linked into layers lying parallel to (024) by C-H⋯O and O-H⋯O inter-actions. The layers inter-act by C-H⋯π and weak aromatic π-π stacking inter-actions [centroid-centroid distances = 3.8476 (16), 3.725 (3) and 3.733 (5) Å].

No MeSH data available.


Related in: MedlinePlus