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Crystal structure of 3-{(E)-[(3,4-di-chloro-phen-yl)imino]-meth-yl}benzene-1,2-diol.

Tahir MN, Shad HA, Rauf A, Khan AH - Acta Crystallogr E Crystallogr Commun (2015)

Bottom Line: In the title Schiff base, C13H9Cl2NO2, which arose from the condensation of 3,4-di-chloro-aniline with 2,3-di-hydroxy-benzaldehyde, the dihedral angle between the aromatic rings is 44.74 (13)°.In the crystal, inversion dimers linked by pairs of O-H⋯O hydrogen bonds generate R 2 (2)(10) loops.A weak C-H⋯π inter-action is also observed.

View Article: PubMed Central - HTML - PubMed

Affiliation: Department of Physics, University of Sargodha, Sargodha, Punjab, Pakistan.

ABSTRACT
In the title Schiff base, C13H9Cl2NO2, which arose from the condensation of 3,4-di-chloro-aniline with 2,3-di-hydroxy-benzaldehyde, the dihedral angle between the aromatic rings is 44.74 (13)°. Intra-molecular O-H⋯O and O-H⋯N hydrogen bonds close S(5) and S(6) rings, respectively. In the crystal, inversion dimers linked by pairs of O-H⋯O hydrogen bonds generate R 2 (2)(10) loops. A weak C-H⋯π inter-action is also observed.

No MeSH data available.


Related in: MedlinePlus

View of the title compound with displacement ellipsoids drawn at the 50% probability level.
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Fap1: View of the title compound with displacement ellipsoids drawn at the 50% probability level.


Crystal structure of 3-{(E)-[(3,4-di-chloro-phen-yl)imino]-meth-yl}benzene-1,2-diol.

Tahir MN, Shad HA, Rauf A, Khan AH - Acta Crystallogr E Crystallogr Commun (2015)

View of the title compound with displacement ellipsoids drawn at the 50% probability level.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC4384559&req=5

Fap1: View of the title compound with displacement ellipsoids drawn at the 50% probability level.
Bottom Line: In the title Schiff base, C13H9Cl2NO2, which arose from the condensation of 3,4-di-chloro-aniline with 2,3-di-hydroxy-benzaldehyde, the dihedral angle between the aromatic rings is 44.74 (13)°.In the crystal, inversion dimers linked by pairs of O-H⋯O hydrogen bonds generate R 2 (2)(10) loops.A weak C-H⋯π inter-action is also observed.

View Article: PubMed Central - HTML - PubMed

Affiliation: Department of Physics, University of Sargodha, Sargodha, Punjab, Pakistan.

ABSTRACT
In the title Schiff base, C13H9Cl2NO2, which arose from the condensation of 3,4-di-chloro-aniline with 2,3-di-hydroxy-benzaldehyde, the dihedral angle between the aromatic rings is 44.74 (13)°. Intra-molecular O-H⋯O and O-H⋯N hydrogen bonds close S(5) and S(6) rings, respectively. In the crystal, inversion dimers linked by pairs of O-H⋯O hydrogen bonds generate R 2 (2)(10) loops. A weak C-H⋯π inter-action is also observed.

No MeSH data available.


Related in: MedlinePlus