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Crystal structure of (Z)-2-hy-droxy-N'-(4-oxo-1,3-thia-zolidin-2-yl-idene)benzohydrazide.

Zhang Y, Li P, Fan X, Jin L - Acta Crystallogr Sect E Struct Rep Online (2014)

Bottom Line: In the title compound, C10H9N3O3S, the five-membered ring adopts a slightly twisted conformation about the Cm-S (m = methyl-ene) bond.The dihedral angle between this ring and the benzene ring is 7.99 (9)°.In the crystal, mol-ecules are linked by N-H⋯O and O-H⋯O hydrogen bonds to generate (001) sheets.

View Article: PubMed Central - HTML - PubMed

Affiliation: College of Chemistry and Material Science, South-Central University for Nationalities, Wuhan 430074, People's Republic of China.

ABSTRACT
In the title compound, C10H9N3O3S, the five-membered ring adopts a slightly twisted conformation about the Cm-S (m = methyl-ene) bond. The dihedral angle between this ring and the benzene ring is 7.99 (9)°. A bifurcated intra-molecular N-H⋯(O,S) hydrogen bond helps to establish the near planar conformation of the mol-ecule. In the crystal, mol-ecules are linked by N-H⋯O and O-H⋯O hydrogen bonds to generate (001) sheets.

No MeSH data available.


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Packing diagram for (I). The hydrogen bonds are indicated by dashed lines.
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Fap2: Packing diagram for (I). The hydrogen bonds are indicated by dashed lines.


Crystal structure of (Z)-2-hy-droxy-N'-(4-oxo-1,3-thia-zolidin-2-yl-idene)benzohydrazide.

Zhang Y, Li P, Fan X, Jin L - Acta Crystallogr Sect E Struct Rep Online (2014)

Packing diagram for (I). The hydrogen bonds are indicated by dashed lines.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC4257235&req=5

Fap2: Packing diagram for (I). The hydrogen bonds are indicated by dashed lines.
Bottom Line: In the title compound, C10H9N3O3S, the five-membered ring adopts a slightly twisted conformation about the Cm-S (m = methyl-ene) bond.The dihedral angle between this ring and the benzene ring is 7.99 (9)°.In the crystal, mol-ecules are linked by N-H⋯O and O-H⋯O hydrogen bonds to generate (001) sheets.

View Article: PubMed Central - HTML - PubMed

Affiliation: College of Chemistry and Material Science, South-Central University for Nationalities, Wuhan 430074, People's Republic of China.

ABSTRACT
In the title compound, C10H9N3O3S, the five-membered ring adopts a slightly twisted conformation about the Cm-S (m = methyl-ene) bond. The dihedral angle between this ring and the benzene ring is 7.99 (9)°. A bifurcated intra-molecular N-H⋯(O,S) hydrogen bond helps to establish the near planar conformation of the mol-ecule. In the crystal, mol-ecules are linked by N-H⋯O and O-H⋯O hydrogen bonds to generate (001) sheets.

No MeSH data available.


Related in: MedlinePlus