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Orphenadrinium dihydrogen citrate.

Kaur M, Jasinski JP, Keeley AC, Yathirajan HS, Siddaraju BP - Acta Crystallogr Sect E Struct Rep Online (2013)

Bottom Line: In the title salt, C(18)H(24)NO(+)·C(6)H(7)O(7) (-), the dihedral angle between the benzene rings in the cation is 74.2 (5)°.In the crystal, anion-anion O-H⋯O hydrogen bonds and weak O-H⋯O inter-actions form infinite chains along [100].Between these chains, cation-anion N-H-O hydrogen bonds are observed, forming an alternate pattern of cation and anion layers and leading to a two-dimensional network parallel to (100).

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Affiliation: Department of Studies in Chemistry, University of Mysore, Manasagangotri, Mysore 570 006, India.

ABSTRACT
In the title salt, C(18)H(24)NO(+)·C(6)H(7)O(7) (-), the dihedral angle between the benzene rings in the cation is 74.2 (5)°. In the crystal, anion-anion O-H⋯O hydrogen bonds and weak O-H⋯O inter-actions form infinite chains along [100]. Between these chains, cation-anion N-H-O hydrogen bonds are observed, forming an alternate pattern of cation and anion layers and leading to a two-dimensional network parallel to (100).

No MeSH data available.


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Packing diagram of the title compound viewed along the c axis. Dashed lines indicate O—H···O anion-anion hydrogen bonds and weak O—H···O intemolecular interactions in concert with cation-anion N—H···O hydrogen bonds forming an infinite two-dimensional network long [100]. The hydrogen atoms not involved in hydrogen bonding have been removed for clarity.
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Fap2: Packing diagram of the title compound viewed along the c axis. Dashed lines indicate O—H···O anion-anion hydrogen bonds and weak O—H···O intemolecular interactions in concert with cation-anion N—H···O hydrogen bonds forming an infinite two-dimensional network long [100]. The hydrogen atoms not involved in hydrogen bonding have been removed for clarity.


Orphenadrinium dihydrogen citrate.

Kaur M, Jasinski JP, Keeley AC, Yathirajan HS, Siddaraju BP - Acta Crystallogr Sect E Struct Rep Online (2013)

Packing diagram of the title compound viewed along the c axis. Dashed lines indicate O—H···O anion-anion hydrogen bonds and weak O—H···O intemolecular interactions in concert with cation-anion N—H···O hydrogen bonds forming an infinite two-dimensional network long [100]. The hydrogen atoms not involved in hydrogen bonding have been removed for clarity.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC3569781&req=5

Fap2: Packing diagram of the title compound viewed along the c axis. Dashed lines indicate O—H···O anion-anion hydrogen bonds and weak O—H···O intemolecular interactions in concert with cation-anion N—H···O hydrogen bonds forming an infinite two-dimensional network long [100]. The hydrogen atoms not involved in hydrogen bonding have been removed for clarity.
Bottom Line: In the title salt, C(18)H(24)NO(+)·C(6)H(7)O(7) (-), the dihedral angle between the benzene rings in the cation is 74.2 (5)°.In the crystal, anion-anion O-H⋯O hydrogen bonds and weak O-H⋯O inter-actions form infinite chains along [100].Between these chains, cation-anion N-H-O hydrogen bonds are observed, forming an alternate pattern of cation and anion layers and leading to a two-dimensional network parallel to (100).

View Article: PubMed Central - HTML - PubMed

Affiliation: Department of Studies in Chemistry, University of Mysore, Manasagangotri, Mysore 570 006, India.

ABSTRACT
In the title salt, C(18)H(24)NO(+)·C(6)H(7)O(7) (-), the dihedral angle between the benzene rings in the cation is 74.2 (5)°. In the crystal, anion-anion O-H⋯O hydrogen bonds and weak O-H⋯O inter-actions form infinite chains along [100]. Between these chains, cation-anion N-H-O hydrogen bonds are observed, forming an alternate pattern of cation and anion layers and leading to a two-dimensional network parallel to (100).

No MeSH data available.


Related in: MedlinePlus