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2-Chloro-N-methyl-N-[2-(methyl-amino)-phen-yl]acetamide.

Bai YB, Chen XH, Ma YT, Zhang AL, Gao JM - Acta Crystallogr Sect E Struct Rep Online (2013)

Bottom Line: The title compound, C(10)H(13)ClN(2)O, was obtained as a by-product in the reaction of 2-chloro-methyl-1H-benzimidazole, dimethyl sulfate and toluene to synthesise 2-chloro-methyl-1-methyl-benzimidazole.The dihedral angle between the benzene ring and the acetamide group is 89.72  (6)° while that between the aromatic ring and the chloracetyl group is 84.40 (4)°.In the crystal, adjacent mol-ecules are linked by pairs of N-H⋯O hydrogen bonds into inversion dimers.

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Affiliation: College of Science, Northwest A&F University, Yangling Shaanxi 712100, People's Republic of China.

ABSTRACT
The title compound, C(10)H(13)ClN(2)O, was obtained as a by-product in the reaction of 2-chloro-methyl-1H-benzimidazole, dimethyl sulfate and toluene to synthesise 2-chloro-methyl-1-methyl-benzimidazole. The dihedral angle between the benzene ring and the acetamide group is 89.72  (6)° while that between the aromatic ring and the chloracetyl group is 84.40 (4)°. In the crystal, adjacent mol-ecules are linked by pairs of N-H⋯O hydrogen bonds into inversion dimers.

No MeSH data available.


The molecular structure of the title compound with labeling and isplacement ellipsoids drawn at the 30% probability level.
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Fap1: The molecular structure of the title compound with labeling and isplacement ellipsoids drawn at the 30% probability level.


2-Chloro-N-methyl-N-[2-(methyl-amino)-phen-yl]acetamide.

Bai YB, Chen XH, Ma YT, Zhang AL, Gao JM - Acta Crystallogr Sect E Struct Rep Online (2013)

The molecular structure of the title compound with labeling and isplacement ellipsoids drawn at the 30% probability level.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC3569763&req=5

Fap1: The molecular structure of the title compound with labeling and isplacement ellipsoids drawn at the 30% probability level.
Bottom Line: The title compound, C(10)H(13)ClN(2)O, was obtained as a by-product in the reaction of 2-chloro-methyl-1H-benzimidazole, dimethyl sulfate and toluene to synthesise 2-chloro-methyl-1-methyl-benzimidazole.The dihedral angle between the benzene ring and the acetamide group is 89.72  (6)° while that between the aromatic ring and the chloracetyl group is 84.40 (4)°.In the crystal, adjacent mol-ecules are linked by pairs of N-H⋯O hydrogen bonds into inversion dimers.

View Article: PubMed Central - HTML - PubMed

Affiliation: College of Science, Northwest A&F University, Yangling Shaanxi 712100, People's Republic of China.

ABSTRACT
The title compound, C(10)H(13)ClN(2)O, was obtained as a by-product in the reaction of 2-chloro-methyl-1H-benzimidazole, dimethyl sulfate and toluene to synthesise 2-chloro-methyl-1-methyl-benzimidazole. The dihedral angle between the benzene ring and the acetamide group is 89.72  (6)° while that between the aromatic ring and the chloracetyl group is 84.40 (4)°. In the crystal, adjacent mol-ecules are linked by pairs of N-H⋯O hydrogen bonds into inversion dimers.

No MeSH data available.