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(2E)-2-(5-Bromo-2-hy-droxy-3-meth-oxy-benzyl-idene)-N-phenyl-hydrazine-carbo-thio-amide.

Jacob JM, Sithambaresan M, Kurup MR - Acta Crystallogr Sect E Struct Rep Online (2012)

Bottom Line: The title compound, C(15)H(14)BrN(3)O(2)S, adopts an E,E conformation with respect to the azomethine and hydrazinic bonds and exists in the thio-amide form.The two rings in the mol-ecule are twisted away from each other, making a dihedral angle of 69.13 (13)°.Intra-molecular N-H⋯N, O-H⋯O and C-H⋯π inter-actions are also present.

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ABSTRACT
The title compound, C(15)H(14)BrN(3)O(2)S, adopts an E,E conformation with respect to the azomethine and hydrazinic bonds and exists in the thio-amide form. The two rings in the mol-ecule are twisted away from each other, making a dihedral angle of 69.13 (13)°. In the crystal, mol-ecules are linked through pairs of N-H⋯O and O-H⋯S hydrogen bonds, leading to the formation of inversion dimers which are stacked along the a axis. Intra-molecular N-H⋯N, O-H⋯O and C-H⋯π inter-actions are also present.

No MeSH data available.


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A view of the unit cell along a axis.
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Fap2: A view of the unit cell along a axis.


(2E)-2-(5-Bromo-2-hy-droxy-3-meth-oxy-benzyl-idene)-N-phenyl-hydrazine-carbo-thio-amide.

Jacob JM, Sithambaresan M, Kurup MR - Acta Crystallogr Sect E Struct Rep Online (2012)

A view of the unit cell along a axis.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC3379435&req=5

Fap2: A view of the unit cell along a axis.
Bottom Line: The title compound, C(15)H(14)BrN(3)O(2)S, adopts an E,E conformation with respect to the azomethine and hydrazinic bonds and exists in the thio-amide form.The two rings in the mol-ecule are twisted away from each other, making a dihedral angle of 69.13 (13)°.Intra-molecular N-H⋯N, O-H⋯O and C-H⋯π inter-actions are also present.

View Article: PubMed Central - HTML - PubMed

ABSTRACT
The title compound, C(15)H(14)BrN(3)O(2)S, adopts an E,E conformation with respect to the azomethine and hydrazinic bonds and exists in the thio-amide form. The two rings in the mol-ecule are twisted away from each other, making a dihedral angle of 69.13 (13)°. In the crystal, mol-ecules are linked through pairs of N-H⋯O and O-H⋯S hydrogen bonds, leading to the formation of inversion dimers which are stacked along the a axis. Intra-molecular N-H⋯N, O-H⋯O and C-H⋯π inter-actions are also present.

No MeSH data available.


Related in: MedlinePlus