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3-{[Bis(pyridin-2-ylmeth-yl)amino]-meth-yl}-2-hy-droxy-5-methyl-benz-aldehyde.

Wang RX, Gao DZ, Ye F, Wu YF, Zhu DR - Acta Crystallogr Sect E Struct Rep Online (2012)

Bottom Line: In the title compound, C(21)H(21)N(3)O(2), the pyridine rings and the benzene ring lie in a propeller arrangement around the central tertiary amine N atom.The dihedral angles formed by the benzene ring with the pyridine rings are 61.0 (3) and 49.6 (3)°, while the dihedral angle between the pyridine rings is 69.7 (3)°.In the crystal, inversion dimers are formed via pairs of C-H⋯N hydrogen bonds.

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Affiliation: College of Chemistry and Chemical Engineering, State Key Laboratory of Materials-Oriented Chemical Engineering, Nanjing University of Technology, Nanjing 210009, People's Republic of China.

ABSTRACT
In the title compound, C(21)H(21)N(3)O(2), the pyridine rings and the benzene ring lie in a propeller arrangement around the central tertiary amine N atom. The dihedral angles formed by the benzene ring with the pyridine rings are 61.0 (3) and 49.6 (3)°, while the dihedral angle between the pyridine rings is 69.7 (3)°. The mol-ecular conformation is stabilized by intramolecular bifurcated O-H⋯N hydrogen bonds. In the crystal, inversion dimers are formed via pairs of C-H⋯N hydrogen bonds.

No MeSH data available.


The molecular structure of the title compound showing displacement ellipsoids drawn at the 30% probability level. Intramolecular hydrogen bonds are drawn as dashed lines.
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Fap1: The molecular structure of the title compound showing displacement ellipsoids drawn at the 30% probability level. Intramolecular hydrogen bonds are drawn as dashed lines.


3-{[Bis(pyridin-2-ylmeth-yl)amino]-meth-yl}-2-hy-droxy-5-methyl-benz-aldehyde.

Wang RX, Gao DZ, Ye F, Wu YF, Zhu DR - Acta Crystallogr Sect E Struct Rep Online (2012)

The molecular structure of the title compound showing displacement ellipsoids drawn at the 30% probability level. Intramolecular hydrogen bonds are drawn as dashed lines.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC3379269&req=5

Fap1: The molecular structure of the title compound showing displacement ellipsoids drawn at the 30% probability level. Intramolecular hydrogen bonds are drawn as dashed lines.
Bottom Line: In the title compound, C(21)H(21)N(3)O(2), the pyridine rings and the benzene ring lie in a propeller arrangement around the central tertiary amine N atom.The dihedral angles formed by the benzene ring with the pyridine rings are 61.0 (3) and 49.6 (3)°, while the dihedral angle between the pyridine rings is 69.7 (3)°.In the crystal, inversion dimers are formed via pairs of C-H⋯N hydrogen bonds.

View Article: PubMed Central - HTML - PubMed

Affiliation: College of Chemistry and Chemical Engineering, State Key Laboratory of Materials-Oriented Chemical Engineering, Nanjing University of Technology, Nanjing 210009, People's Republic of China.

ABSTRACT
In the title compound, C(21)H(21)N(3)O(2), the pyridine rings and the benzene ring lie in a propeller arrangement around the central tertiary amine N atom. The dihedral angles formed by the benzene ring with the pyridine rings are 61.0 (3) and 49.6 (3)°, while the dihedral angle between the pyridine rings is 69.7 (3)°. The mol-ecular conformation is stabilized by intramolecular bifurcated O-H⋯N hydrogen bonds. In the crystal, inversion dimers are formed via pairs of C-H⋯N hydrogen bonds.

No MeSH data available.