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Nickel alendronate.

Sikorska M, Gazda M, Chojnacki J - Acta Crystallogr Sect E Struct Rep Online (2012)

Bottom Line: The title compound {sys-tematic name: bis(μ(2)-dihydrogen 4-aza-niumyl-1-hy-droxy-butane-1,1-di-phos-pho-n-ato)bis-[aqua-(dihydrogen 4-aza-nium-yl-1-hy-droxy-butane-1,1-diphospho-n-ato)nickel(II)] dihydrate}, [Ni(2)(C(4)H(12)NO(7)P(2))(4)(H(2)O)(2)]·2H(2)O, was synthesiized under hydro-thermal conditions.Its structure is isotypic with the Co(II) analogue.One water mol-ecule is bound to the Ni(II) atom in the octahedral coordination sphere, while the second is part of the inter-molecular hydrogen-bond system.

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ABSTRACT
The title compound {sys-tematic name: bis(μ(2)-dihydrogen 4-aza-niumyl-1-hy-droxy-butane-1,1-di-phos-pho-n-ato)bis-[aqua-(dihydrogen 4-aza-nium-yl-1-hy-droxy-butane-1,1-diphospho-n-ato)nickel(II)] dihydrate}, [Ni(2)(C(4)H(12)NO(7)P(2))(4)(H(2)O)(2)]·2H(2)O, was synthesiized under hydro-thermal conditions. Its structure is isotypic with the Co(II) analogue. The crystal structure is built up from centrosymmetric dinuclear complex mol-ecules and the structure is reinforced by a net of inter-molecular O-H⋯O and N-H⋯O hydrogen bonds. One water mol-ecule is bound to the Ni(II) atom in the octahedral coordination sphere, while the second is part of the inter-molecular hydrogen-bond system.

No MeSH data available.


Related in: MedlinePlus

Packing diagram for C16H52N4Ni2O30P8 viewed along the b axis. Please note influence of different bending of the alkylammonium groups on hydrogen bonding system. Colours: central molecule - grey, molecules linked by N1—H···O5 bond - red, other neighbour molecules - blue
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Fap2: Packing diagram for C16H52N4Ni2O30P8 viewed along the b axis. Please note influence of different bending of the alkylammonium groups on hydrogen bonding system. Colours: central molecule - grey, molecules linked by N1—H···O5 bond - red, other neighbour molecules - blue


Nickel alendronate.

Sikorska M, Gazda M, Chojnacki J - Acta Crystallogr Sect E Struct Rep Online (2012)

Packing diagram for C16H52N4Ni2O30P8 viewed along the b axis. Please note influence of different bending of the alkylammonium groups on hydrogen bonding system. Colours: central molecule - grey, molecules linked by N1—H···O5 bond - red, other neighbour molecules - blue
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC3379142&req=5

Fap2: Packing diagram for C16H52N4Ni2O30P8 viewed along the b axis. Please note influence of different bending of the alkylammonium groups on hydrogen bonding system. Colours: central molecule - grey, molecules linked by N1—H···O5 bond - red, other neighbour molecules - blue
Bottom Line: The title compound {sys-tematic name: bis(μ(2)-dihydrogen 4-aza-niumyl-1-hy-droxy-butane-1,1-di-phos-pho-n-ato)bis-[aqua-(dihydrogen 4-aza-nium-yl-1-hy-droxy-butane-1,1-diphospho-n-ato)nickel(II)] dihydrate}, [Ni(2)(C(4)H(12)NO(7)P(2))(4)(H(2)O)(2)]·2H(2)O, was synthesiized under hydro-thermal conditions.Its structure is isotypic with the Co(II) analogue.One water mol-ecule is bound to the Ni(II) atom in the octahedral coordination sphere, while the second is part of the inter-molecular hydrogen-bond system.

View Article: PubMed Central - HTML - PubMed

ABSTRACT
The title compound {sys-tematic name: bis(μ(2)-dihydrogen 4-aza-niumyl-1-hy-droxy-butane-1,1-di-phos-pho-n-ato)bis-[aqua-(dihydrogen 4-aza-nium-yl-1-hy-droxy-butane-1,1-diphospho-n-ato)nickel(II)] dihydrate}, [Ni(2)(C(4)H(12)NO(7)P(2))(4)(H(2)O)(2)]·2H(2)O, was synthesiized under hydro-thermal conditions. Its structure is isotypic with the Co(II) analogue. The crystal structure is built up from centrosymmetric dinuclear complex mol-ecules and the structure is reinforced by a net of inter-molecular O-H⋯O and N-H⋯O hydrogen bonds. One water mol-ecule is bound to the Ni(II) atom in the octahedral coordination sphere, while the second is part of the inter-molecular hydrogen-bond system.

No MeSH data available.


Related in: MedlinePlus