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Bis(N-methyl-N-phenyl-carbamo-yl)disulfane.

Schroll AL, Pink M, Barany G - Acta Crystallogr Sect E Struct Rep Online (2012)

Bottom Line: The title compound, C(16)H(16)N(2)O(2)S(2), has been synthesized by several different high-yield routes, and has been encountered as a co-product in a number of reaction pathways, ever since it became of inter-est to our research program over 30 years ago.We now confirm the proposed mol-ecular structure in which the mol-ecule exhibits a twofold axis of symmetry through the mid-point of the S-S bond and the two planes defined by the (carbamo-yl)sulfenyl moieties are essentially perpendicular to each other [dihedral angle = 81.55 (14)°].

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ABSTRACT
The title compound, C(16)H(16)N(2)O(2)S(2), has been synthesized by several different high-yield routes, and has been encountered as a co-product in a number of reaction pathways, ever since it became of inter-est to our research program over 30 years ago. We now confirm the proposed mol-ecular structure in which the mol-ecule exhibits a twofold axis of symmetry through the mid-point of the S-S bond and the two planes defined by the (carbamo-yl)sulfenyl moieties are essentially perpendicular to each other [dihedral angle = 81.55 (14)°].

No MeSH data available.


Crystallographic structure of the title compound showing 50% probability displacement ellipsoids and with all non-hydrogen atoms labelled and numbered.
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Fap1: Crystallographic structure of the title compound showing 50% probability displacement ellipsoids and with all non-hydrogen atoms labelled and numbered.


Bis(N-methyl-N-phenyl-carbamo-yl)disulfane.

Schroll AL, Pink M, Barany G - Acta Crystallogr Sect E Struct Rep Online (2012)

Crystallographic structure of the title compound showing 50% probability displacement ellipsoids and with all non-hydrogen atoms labelled and numbered.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC3344649&req=5

Fap1: Crystallographic structure of the title compound showing 50% probability displacement ellipsoids and with all non-hydrogen atoms labelled and numbered.
Bottom Line: The title compound, C(16)H(16)N(2)O(2)S(2), has been synthesized by several different high-yield routes, and has been encountered as a co-product in a number of reaction pathways, ever since it became of inter-est to our research program over 30 years ago.We now confirm the proposed mol-ecular structure in which the mol-ecule exhibits a twofold axis of symmetry through the mid-point of the S-S bond and the two planes defined by the (carbamo-yl)sulfenyl moieties are essentially perpendicular to each other [dihedral angle = 81.55 (14)°].

View Article: PubMed Central - HTML - PubMed

ABSTRACT
The title compound, C(16)H(16)N(2)O(2)S(2), has been synthesized by several different high-yield routes, and has been encountered as a co-product in a number of reaction pathways, ever since it became of inter-est to our research program over 30 years ago. We now confirm the proposed mol-ecular structure in which the mol-ecule exhibits a twofold axis of symmetry through the mid-point of the S-S bond and the two planes defined by the (carbamo-yl)sulfenyl moieties are essentially perpendicular to each other [dihedral angle = 81.55 (14)°].

No MeSH data available.