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N'-[(E)-4-Benz-yloxy-2-hy-droxy-benzyl-idene]-4-nitro-benzohydrazide monohydrate.

Joseph B, Sithambaresan M, Kurup MR - Acta Crystallogr Sect E Struct Rep Online (2012)

Bottom Line: A water mol-ecule of solvation is present in the lattice.Inter-molecular O-H⋯O, N-H⋯O and C-H⋯O hydrogen-bonding inter-actions establish a supra-molecular linkage among the mol-ecules in the crystal structure.There are also C-H⋯π inter-actions present.

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ABSTRACT
The title compound, C(21)H(17)N(3)O(5)·H(2)O, exists in the keto form with an E conformation with respect to the azomethine double bond. The twist angles between the aromatic rings are in the range 4.67 (10)-17.54 (10)°. A water mol-ecule of solvation is present in the lattice. A conventional intra-molecular O-H⋯N hydrogen bond increases the rigidity of the mol-ecule. Inter-molecular O-H⋯O, N-H⋯O and C-H⋯O hydrogen-bonding inter-actions establish a supra-molecular linkage among the mol-ecules in the crystal structure. There are also C-H⋯π inter-actions present.

No MeSH data available.


Related in: MedlinePlus

Packing arrangement of molecules along a axis.
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Fap4: Packing arrangement of molecules along a axis.


N'-[(E)-4-Benz-yloxy-2-hy-droxy-benzyl-idene]-4-nitro-benzohydrazide monohydrate.

Joseph B, Sithambaresan M, Kurup MR - Acta Crystallogr Sect E Struct Rep Online (2012)

Packing arrangement of molecules along a axis.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC3344544&req=5

Fap4: Packing arrangement of molecules along a axis.
Bottom Line: A water mol-ecule of solvation is present in the lattice.Inter-molecular O-H⋯O, N-H⋯O and C-H⋯O hydrogen-bonding inter-actions establish a supra-molecular linkage among the mol-ecules in the crystal structure.There are also C-H⋯π inter-actions present.

View Article: PubMed Central - HTML - PubMed

ABSTRACT
The title compound, C(21)H(17)N(3)O(5)·H(2)O, exists in the keto form with an E conformation with respect to the azomethine double bond. The twist angles between the aromatic rings are in the range 4.67 (10)-17.54 (10)°. A water mol-ecule of solvation is present in the lattice. A conventional intra-molecular O-H⋯N hydrogen bond increases the rigidity of the mol-ecule. Inter-molecular O-H⋯O, N-H⋯O and C-H⋯O hydrogen-bonding inter-actions establish a supra-molecular linkage among the mol-ecules in the crystal structure. There are also C-H⋯π inter-actions present.

No MeSH data available.


Related in: MedlinePlus