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5-Benzoyl-13-bromo-4-hy-droxy[2.2]paracyclo-phane.

Ma K, Duan W, He F, Ma Y - Acta Crystallogr Sect E Struct Rep Online (2012)

Bottom Line: The title compound, C(23)H(19)BrO(2), was synthesized from 13-bromo-4-hy-droxy[2.2]paracyclo-phane and benzoyl chloride.The hy-droxy and carbonyl groups are involved in intra-molecular O-H⋯O hydrogen bonding.The crystal packing exhibits weak C-H⋯O inter-actions, which link the mol-ecules into sheets parallel to the bc plane.

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ABSTRACT
The title compound, C(23)H(19)BrO(2), was synthesized from 13-bromo-4-hy-droxy[2.2]paracyclo-phane and benzoyl chloride. The hy-droxy and carbonyl groups are involved in intra-molecular O-H⋯O hydrogen bonding. The crystal packing exhibits weak C-H⋯O inter-actions, which link the mol-ecules into sheets parallel to the bc plane.

No MeSH data available.


The molecular structure of (I) showing the atom numbering scheme and 50% probabilty displacement ellipsoids. The H atoms are omitted for clarity.
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Fap1: The molecular structure of (I) showing the atom numbering scheme and 50% probabilty displacement ellipsoids. The H atoms are omitted for clarity.


5-Benzoyl-13-bromo-4-hy-droxy[2.2]paracyclo-phane.

Ma K, Duan W, He F, Ma Y - Acta Crystallogr Sect E Struct Rep Online (2012)

The molecular structure of (I) showing the atom numbering scheme and 50% probabilty displacement ellipsoids. The H atoms are omitted for clarity.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC3344509&req=5

Fap1: The molecular structure of (I) showing the atom numbering scheme and 50% probabilty displacement ellipsoids. The H atoms are omitted for clarity.
Bottom Line: The title compound, C(23)H(19)BrO(2), was synthesized from 13-bromo-4-hy-droxy[2.2]paracyclo-phane and benzoyl chloride.The hy-droxy and carbonyl groups are involved in intra-molecular O-H⋯O hydrogen bonding.The crystal packing exhibits weak C-H⋯O inter-actions, which link the mol-ecules into sheets parallel to the bc plane.

View Article: PubMed Central - HTML - PubMed

ABSTRACT
The title compound, C(23)H(19)BrO(2), was synthesized from 13-bromo-4-hy-droxy[2.2]paracyclo-phane and benzoyl chloride. The hy-droxy and carbonyl groups are involved in intra-molecular O-H⋯O hydrogen bonding. The crystal packing exhibits weak C-H⋯O inter-actions, which link the mol-ecules into sheets parallel to the bc plane.

No MeSH data available.