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N'-(3-Fluoro-benzyl-idene)-4-hy-droxy-3-meth-oxy-benzohydrazide methanol monosolvate.

Zong QS - Acta Crystallogr Sect E Struct Rep Online (2012)

Bottom Line: In the title compound, C(15)H(13)FN(2)O(3)·CH(3)OH, the dihedral angle between the benzene rings of the benzohydrazone mol-ecule is 5.3 (3)°.The C atom of the meth-oxy group is almost coplanar with its attached ring [deviation = 0.017 (2) Å].The r.m.s. deviation of the 21 non-H atoms of the hydrazone mol-ecule is 0.106 Å.

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Affiliation: College of Biology and Chemical Engineering, Jiaxing University, Jiaxing Zhejiang 314001, People's Republic of China, and School of Pharmaceutical Sciences, Zhejiang University, Hangzhou Zhejiang 310058, People's Republic of China.

ABSTRACT
In the title compound, C(15)H(13)FN(2)O(3)·CH(3)OH, the dihedral angle between the benzene rings of the benzohydrazone mol-ecule is 5.3 (3)°. The C atom of the meth-oxy group is almost coplanar with its attached ring [deviation = 0.017 (2) Å]. The r.m.s. deviation of the 21 non-H atoms of the hydrazone mol-ecule is 0.106 Å. In the crystal, the components are linked by O(m)-H⋯O(h), N(h)-H⋯O(m) and O(h)-H⋯O(h) (m = methanol and h = hydrazone) hydrogen bonds, forming (001) layers.

No MeSH data available.


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The crystal structure of the title compound, viewed along a axis. Hydrogen bonds are shown as dashed lines.
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Fap2: The crystal structure of the title compound, viewed along a axis. Hydrogen bonds are shown as dashed lines.


N'-(3-Fluoro-benzyl-idene)-4-hy-droxy-3-meth-oxy-benzohydrazide methanol monosolvate.

Zong QS - Acta Crystallogr Sect E Struct Rep Online (2012)

The crystal structure of the title compound, viewed along a axis. Hydrogen bonds are shown as dashed lines.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC3344474&req=5

Fap2: The crystal structure of the title compound, viewed along a axis. Hydrogen bonds are shown as dashed lines.
Bottom Line: In the title compound, C(15)H(13)FN(2)O(3)·CH(3)OH, the dihedral angle between the benzene rings of the benzohydrazone mol-ecule is 5.3 (3)°.The C atom of the meth-oxy group is almost coplanar with its attached ring [deviation = 0.017 (2) Å].The r.m.s. deviation of the 21 non-H atoms of the hydrazone mol-ecule is 0.106 Å.

View Article: PubMed Central - HTML - PubMed

Affiliation: College of Biology and Chemical Engineering, Jiaxing University, Jiaxing Zhejiang 314001, People's Republic of China, and School of Pharmaceutical Sciences, Zhejiang University, Hangzhou Zhejiang 310058, People's Republic of China.

ABSTRACT
In the title compound, C(15)H(13)FN(2)O(3)·CH(3)OH, the dihedral angle between the benzene rings of the benzohydrazone mol-ecule is 5.3 (3)°. The C atom of the meth-oxy group is almost coplanar with its attached ring [deviation = 0.017 (2) Å]. The r.m.s. deviation of the 21 non-H atoms of the hydrazone mol-ecule is 0.106 Å. In the crystal, the components are linked by O(m)-H⋯O(h), N(h)-H⋯O(m) and O(h)-H⋯O(h) (m = methanol and h = hydrazone) hydrogen bonds, forming (001) layers.

No MeSH data available.


Related in: MedlinePlus