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1-(2-Meth-oxy-phen-yl)-2-{[2-(2-meth-oxy-phen-yl)hydrazinyl-idene](nitro)-meth-yl}diazene.

von Eschwege KG, Muller F, Hill TN - Acta Crystallogr Sect E Struct Rep Online (2012)

Bottom Line: In the title compound, C(15)H(15)N(5)O(4), a nitro-formazan derivative, the formazan unit is essentially planar with an r.m.s. deviation of 0.0204 (6) Å and adopts a closed syn,s-cis configuration with an intra-molecular N-H⋯N hydrogen bond.The formazan plane makes dihedral angles of 4.32 (5) and 24.35 (5)° with the benzene rings.The dihedral angle between the formazan plane and the nitro group is 12.58 (8)°.

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Affiliation: Department of Chemistry, University of the Free State, PO Box 339, Bloemfontein 9300, South Africa.

ABSTRACT
In the title compound, C(15)H(15)N(5)O(4), a nitro-formazan derivative, the formazan unit is essentially planar with an r.m.s. deviation of 0.0204 (6) Å and adopts a closed syn,s-cis configuration with an intra-molecular N-H⋯N hydrogen bond. The formazan plane makes dihedral angles of 4.32 (5) and 24.35 (5)° with the benzene rings. The dihedral angle between the formazan plane and the nitro group is 12.58 (8)°. In the crystal, C-H⋯O inter-actions connect the mol-ecules into an inversion dimer.

No MeSH data available.


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A packing diagram of the title compound, illustrating the parallel sheet configuration as viewed along the b axis.
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Fap3: A packing diagram of the title compound, illustrating the parallel sheet configuration as viewed along the b axis.


1-(2-Meth-oxy-phen-yl)-2-{[2-(2-meth-oxy-phen-yl)hydrazinyl-idene](nitro)-meth-yl}diazene.

von Eschwege KG, Muller F, Hill TN - Acta Crystallogr Sect E Struct Rep Online (2012)

A packing diagram of the title compound, illustrating the parallel sheet configuration as viewed along the b axis.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC3295411&req=5

Fap3: A packing diagram of the title compound, illustrating the parallel sheet configuration as viewed along the b axis.
Bottom Line: In the title compound, C(15)H(15)N(5)O(4), a nitro-formazan derivative, the formazan unit is essentially planar with an r.m.s. deviation of 0.0204 (6) Å and adopts a closed syn,s-cis configuration with an intra-molecular N-H⋯N hydrogen bond.The formazan plane makes dihedral angles of 4.32 (5) and 24.35 (5)° with the benzene rings.The dihedral angle between the formazan plane and the nitro group is 12.58 (8)°.

View Article: PubMed Central - HTML - PubMed

Affiliation: Department of Chemistry, University of the Free State, PO Box 339, Bloemfontein 9300, South Africa.

ABSTRACT
In the title compound, C(15)H(15)N(5)O(4), a nitro-formazan derivative, the formazan unit is essentially planar with an r.m.s. deviation of 0.0204 (6) Å and adopts a closed syn,s-cis configuration with an intra-molecular N-H⋯N hydrogen bond. The formazan plane makes dihedral angles of 4.32 (5) and 24.35 (5)° with the benzene rings. The dihedral angle between the formazan plane and the nitro group is 12.58 (8)°. In the crystal, C-H⋯O inter-actions connect the mol-ecules into an inversion dimer.

No MeSH data available.


Related in: MedlinePlus