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2-[(E)-2-Hy-droxy-5-(trifluoro-meth-oxy)benzyl-idene-amino]-4-methyl-phenol.

Karadağ AT, Atalay S, Genç H - Acta Crystallogr Sect E Struct Rep Online (2010)

Bottom Line: The F atoms of the -CF(3) group are disordered over two sets of sites with refined occupancies of 0.61 (5) and 0.39 (5).An intra-molecular N-H⋯O hydrogen bond occurs.The crystal structure is stabilized by inter-molecular O-H⋯O hydrogen bonds.

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ABSTRACT
The title compound, C(15)H(12)F(3)NO(3), is a Schiff base which adopts the cis-quinoid form in the solid state. The dihedral angle between the least-squares planes of the benzene rings being 3.6 (1)°. The F atoms of the -CF(3) group are disordered over two sets of sites with refined occupancies of 0.61 (5) and 0.39 (5). An intra-molecular N-H⋯O hydrogen bond occurs. The crystal structure is stabilized by inter-molecular O-H⋯O hydrogen bonds.

No MeSH data available.


Partial packing view showing the O—H···O hydrogen bonds represented as dashed lines [symmetry code: (i)-x, -y + 2, -z + 1].
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Fap2: Partial packing view showing the O—H···O hydrogen bonds represented as dashed lines [symmetry code: (i)-x, -y + 2, -z + 1].


2-[(E)-2-Hy-droxy-5-(trifluoro-meth-oxy)benzyl-idene-amino]-4-methyl-phenol.

Karadağ AT, Atalay S, Genç H - Acta Crystallogr Sect E Struct Rep Online (2010)

Partial packing view showing the O—H···O hydrogen bonds represented as dashed lines [symmetry code: (i)-x, -y + 2, -z + 1].
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC3050197&req=5

Fap2: Partial packing view showing the O—H···O hydrogen bonds represented as dashed lines [symmetry code: (i)-x, -y + 2, -z + 1].
Bottom Line: The F atoms of the -CF(3) group are disordered over two sets of sites with refined occupancies of 0.61 (5) and 0.39 (5).An intra-molecular N-H⋯O hydrogen bond occurs.The crystal structure is stabilized by inter-molecular O-H⋯O hydrogen bonds.

View Article: PubMed Central - HTML - PubMed

ABSTRACT
The title compound, C(15)H(12)F(3)NO(3), is a Schiff base which adopts the cis-quinoid form in the solid state. The dihedral angle between the least-squares planes of the benzene rings being 3.6 (1)°. The F atoms of the -CF(3) group are disordered over two sets of sites with refined occupancies of 0.61 (5) and 0.39 (5). An intra-molecular N-H⋯O hydrogen bond occurs. The crystal structure is stabilized by inter-molecular O-H⋯O hydrogen bonds.

No MeSH data available.