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Chlorido[1-(4,5-dihydro-1,3-thia-zol-2-yl-κN)ethanone thio-semicarbazonato-κN,S]nickel(II).

Viñuelas-Zahínos E, Luna-Giles F, Torres-García P, Bernalte-García A - Acta Crystallogr Sect E Struct Rep Online (2010)

Bottom Line: In the title compound, [Ni(C(6)H(9)N(4)S(2))Cl], the Ni atom is in a slightly distorted square-planar environment coordinated by a Cl atom and a deprotonated thio-semicarbazone ligand via its thia-zoline N, azomethine N and thiol-ate S atoms.Short inter-molecular N-H⋯Cl and C-H⋯S contacts are present in the crystal structure.

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Affiliation: Departamento de Quimica Organica e Inorganica, Facultad de Ciencias, Universidad de Extremadura, Badajoz, Spain.

ABSTRACT
In the title compound, [Ni(C(6)H(9)N(4)S(2))Cl], the Ni atom is in a slightly distorted square-planar environment coordinated by a Cl atom and a deprotonated thio-semicarbazone ligand via its thia-zoline N, azomethine N and thiol-ate S atoms. Short inter-molecular N-H⋯Cl and C-H⋯S contacts are present in the crystal structure.

No MeSH data available.


A view of molecular structure of title compound, showing the atom–numbering scheme. Displacement ellipsoids are drawn at 50% probability level. H atoms are presented as a small spheres of arbitrary radius.
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Fap1: A view of molecular structure of title compound, showing the atom–numbering scheme. Displacement ellipsoids are drawn at 50% probability level. H atoms are presented as a small spheres of arbitrary radius.


Chlorido[1-(4,5-dihydro-1,3-thia-zol-2-yl-κN)ethanone thio-semicarbazonato-κN,S]nickel(II).

Viñuelas-Zahínos E, Luna-Giles F, Torres-García P, Bernalte-García A - Acta Crystallogr Sect E Struct Rep Online (2010)

A view of molecular structure of title compound, showing the atom–numbering scheme. Displacement ellipsoids are drawn at 50% probability level. H atoms are presented as a small spheres of arbitrary radius.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC3050191&req=5

Fap1: A view of molecular structure of title compound, showing the atom–numbering scheme. Displacement ellipsoids are drawn at 50% probability level. H atoms are presented as a small spheres of arbitrary radius.
Bottom Line: In the title compound, [Ni(C(6)H(9)N(4)S(2))Cl], the Ni atom is in a slightly distorted square-planar environment coordinated by a Cl atom and a deprotonated thio-semicarbazone ligand via its thia-zoline N, azomethine N and thiol-ate S atoms.Short inter-molecular N-H⋯Cl and C-H⋯S contacts are present in the crystal structure.

View Article: PubMed Central - HTML - PubMed

Affiliation: Departamento de Quimica Organica e Inorganica, Facultad de Ciencias, Universidad de Extremadura, Badajoz, Spain.

ABSTRACT
In the title compound, [Ni(C(6)H(9)N(4)S(2))Cl], the Ni atom is in a slightly distorted square-planar environment coordinated by a Cl atom and a deprotonated thio-semicarbazone ligand via its thia-zoline N, azomethine N and thiol-ate S atoms. Short inter-molecular N-H⋯Cl and C-H⋯S contacts are present in the crystal structure.

No MeSH data available.