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5-[(E)-Benzyl-idene]-2-hy-droxy-10-methyl-8-phenyl-3,10-diazahexa-cyclo-[10.7.1.1.0.0.0]henicosa-1(19),12(20),13,15,17-pentaen-6-one ethanol 0.25-solvate 0.6-hydrate.

Kumar RS, Osman H, Perumal S, Hemamalini M, Fun HK - Acta Crystallogr Sect E Struct Rep Online (2010)

Bottom Line: In the title compound, C(33)H(28)N(2)O(2)·0.25C(2)H(6)O·0.6H(2)O, the piperidone ring adopts a chair conformation and the pyrrolidine ring adopts an envelope conformation.The dihedral angle between the two phenyl rings is 70.83 (16)°.In the crystal, mol-ecules are connected by inter-molecular O-H⋯O and C-H⋯O hydrogen bonds, forming a three-dimensional network.

View Article: PubMed Central - HTML - PubMed

ABSTRACT
In the title compound, C(33)H(28)N(2)O(2)·0.25C(2)H(6)O·0.6H(2)O, the piperidone ring adopts a chair conformation and the pyrrolidine ring adopts an envelope conformation. The dihedral angle between the two phenyl rings is 70.83 (16)°. One of the N atoms of the organic mol-ecule is disordered over two positions in a 0.52 (4):0.48 (4) ratio and the two solvent mol-ecules are partially occupied and show high displacement parameters. In the crystal, mol-ecules are connected by inter-molecular O-H⋯O and C-H⋯O hydrogen bonds, forming a three-dimensional network.

No MeSH data available.


Related in: MedlinePlus

The crystal packing of (I), showing hydrogen-bonded (dashed lines) network. Solvent molecules, minor disorder components and H atoms are not involing the hydrogen bond interactions are omitted for clarity.
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Fap2: The crystal packing of (I), showing hydrogen-bonded (dashed lines) network. Solvent molecules, minor disorder components and H atoms are not involing the hydrogen bond interactions are omitted for clarity.


5-[(E)-Benzyl-idene]-2-hy-droxy-10-methyl-8-phenyl-3,10-diazahexa-cyclo-[10.7.1.1.0.0.0]henicosa-1(19),12(20),13,15,17-pentaen-6-one ethanol 0.25-solvate 0.6-hydrate.

Kumar RS, Osman H, Perumal S, Hemamalini M, Fun HK - Acta Crystallogr Sect E Struct Rep Online (2010)

The crystal packing of (I), showing hydrogen-bonded (dashed lines) network. Solvent molecules, minor disorder components and H atoms are not involing the hydrogen bond interactions are omitted for clarity.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC3009066&req=5

Fap2: The crystal packing of (I), showing hydrogen-bonded (dashed lines) network. Solvent molecules, minor disorder components and H atoms are not involing the hydrogen bond interactions are omitted for clarity.
Bottom Line: In the title compound, C(33)H(28)N(2)O(2)·0.25C(2)H(6)O·0.6H(2)O, the piperidone ring adopts a chair conformation and the pyrrolidine ring adopts an envelope conformation.The dihedral angle between the two phenyl rings is 70.83 (16)°.In the crystal, mol-ecules are connected by inter-molecular O-H⋯O and C-H⋯O hydrogen bonds, forming a three-dimensional network.

View Article: PubMed Central - HTML - PubMed

ABSTRACT
In the title compound, C(33)H(28)N(2)O(2)·0.25C(2)H(6)O·0.6H(2)O, the piperidone ring adopts a chair conformation and the pyrrolidine ring adopts an envelope conformation. The dihedral angle between the two phenyl rings is 70.83 (16)°. One of the N atoms of the organic mol-ecule is disordered over two positions in a 0.52 (4):0.48 (4) ratio and the two solvent mol-ecules are partially occupied and show high displacement parameters. In the crystal, mol-ecules are connected by inter-molecular O-H⋯O and C-H⋯O hydrogen bonds, forming a three-dimensional network.

No MeSH data available.


Related in: MedlinePlus