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Butane-1,2,3,4-tetra-carboxylic acid-4,4'-bipyridine (1/2).

Zhang N, Shi XM, Shao M, Li MX - Acta Crystallogr Sect E Struct Rep Online (2009)

Bottom Line: The hydro-thermal reaction of butane-1,2,3,4-tetra-carboxylic acid (H(4)butca), 4,4'-bipyridine (bipy) and Mn(SO(4))(2)·H(2)O afforded a new co-crystal, C(8)H(10)O(8)·2C(10)H(8)N(2) or H(4)butca·2(bipy), in which strong O-H⋯N hydrogen-bonding and weak π-π stacking [centroid-centroid distance = 3.8459 (19) Å] inter-actions assemble the organic mol-ecules into a three-dimensional supra-molecular framework.C-H⋯O inter-actions are also present.The whole mol-ecule has inversion symmetry.

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ABSTRACT
The hydro-thermal reaction of butane-1,2,3,4-tetra-carboxylic acid (H(4)butca), 4,4'-bipyridine (bipy) and Mn(SO(4))(2)·H(2)O afforded a new co-crystal, C(8)H(10)O(8)·2C(10)H(8)N(2) or H(4)butca·2(bipy), in which strong O-H⋯N hydrogen-bonding and weak π-π stacking [centroid-centroid distance = 3.8459 (19) Å] inter-actions assemble the organic mol-ecules into a three-dimensional supra-molecular framework. C-H⋯O inter-actions are also present. The whole mol-ecule has inversion symmetry.

No MeSH data available.


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Crystal packing diagram of compound (I)
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Fap2: Crystal packing diagram of compound (I)


Butane-1,2,3,4-tetra-carboxylic acid-4,4'-bipyridine (1/2).

Zhang N, Shi XM, Shao M, Li MX - Acta Crystallogr Sect E Struct Rep Online (2009)

Crystal packing diagram of compound (I)
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC2977318&req=5

Fap2: Crystal packing diagram of compound (I)
Bottom Line: The hydro-thermal reaction of butane-1,2,3,4-tetra-carboxylic acid (H(4)butca), 4,4'-bipyridine (bipy) and Mn(SO(4))(2)·H(2)O afforded a new co-crystal, C(8)H(10)O(8)·2C(10)H(8)N(2) or H(4)butca·2(bipy), in which strong O-H⋯N hydrogen-bonding and weak π-π stacking [centroid-centroid distance = 3.8459 (19) Å] inter-actions assemble the organic mol-ecules into a three-dimensional supra-molecular framework.C-H⋯O inter-actions are also present.The whole mol-ecule has inversion symmetry.

View Article: PubMed Central - HTML - PubMed

ABSTRACT
The hydro-thermal reaction of butane-1,2,3,4-tetra-carboxylic acid (H(4)butca), 4,4'-bipyridine (bipy) and Mn(SO(4))(2)·H(2)O afforded a new co-crystal, C(8)H(10)O(8)·2C(10)H(8)N(2) or H(4)butca·2(bipy), in which strong O-H⋯N hydrogen-bonding and weak π-π stacking [centroid-centroid distance = 3.8459 (19) Å] inter-actions assemble the organic mol-ecules into a three-dimensional supra-molecular framework. C-H⋯O inter-actions are also present. The whole mol-ecule has inversion symmetry.

No MeSH data available.


Related in: MedlinePlus