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2,4,6,8-Tetra-kis(2-methoxy-phen-yl)-3,7-diaza-bicyclo-[3.3.1]nonan-9-one diethyl ether hemisolvate.

Fun HK, Yeap CS, Rajesh K, Sarveswari S, Vijayakumar V - Acta Crystallogr Sect E Struct Rep Online (2009)

Bottom Line: Two intra-molecular N-H⋯O hydrogen bonds generate S(6) ring motifs.The bicyclo-[3.3.1]nonane ring system adopts a chair-boat conformation.In the crystal structure, the mol-ecules are linked by weak inter-molecular C-H⋯N hydro-gen bonds into chains along the b axis; additional stabilization is provide by C-H⋯π inter-actions.

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ABSTRACT
In the title compound, C(35)H(36)N(2)O(5)·0.5C(4)H(10)O, the asymmetric unit contains one bicyclo-[3.3.1]nonane mol-ecule and a half-occupancy diethyl ether solvent with the O atom lying on a crystallographic inversion center. Two intra-molecular N-H⋯O hydrogen bonds generate S(6) ring motifs. The bicyclo-[3.3.1]nonane ring system adopts a chair-boat conformation. In the crystal structure, the mol-ecules are linked by weak inter-molecular C-H⋯N hydro-gen bonds into chains along the b axis; additional stabilization is provide by C-H⋯π inter-actions.

No MeSH data available.


Related in: MedlinePlus

The crystal packing of title compound, showing the molecules linked along the b axis. The solvent molecules are omitted for clarity. Intermolecular hydrogen bonds are shown as dashed lines.
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Fap2: The crystal packing of title compound, showing the molecules linked along the b axis. The solvent molecules are omitted for clarity. Intermolecular hydrogen bonds are shown as dashed lines.


2,4,6,8-Tetra-kis(2-methoxy-phen-yl)-3,7-diaza-bicyclo-[3.3.1]nonan-9-one diethyl ether hemisolvate.

Fun HK, Yeap CS, Rajesh K, Sarveswari S, Vijayakumar V - Acta Crystallogr Sect E Struct Rep Online (2009)

The crystal packing of title compound, showing the molecules linked along the b axis. The solvent molecules are omitted for clarity. Intermolecular hydrogen bonds are shown as dashed lines.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC2970300&req=5

Fap2: The crystal packing of title compound, showing the molecules linked along the b axis. The solvent molecules are omitted for clarity. Intermolecular hydrogen bonds are shown as dashed lines.
Bottom Line: Two intra-molecular N-H⋯O hydrogen bonds generate S(6) ring motifs.The bicyclo-[3.3.1]nonane ring system adopts a chair-boat conformation.In the crystal structure, the mol-ecules are linked by weak inter-molecular C-H⋯N hydro-gen bonds into chains along the b axis; additional stabilization is provide by C-H⋯π inter-actions.

View Article: PubMed Central - HTML - PubMed

ABSTRACT
In the title compound, C(35)H(36)N(2)O(5)·0.5C(4)H(10)O, the asymmetric unit contains one bicyclo-[3.3.1]nonane mol-ecule and a half-occupancy diethyl ether solvent with the O atom lying on a crystallographic inversion center. Two intra-molecular N-H⋯O hydrogen bonds generate S(6) ring motifs. The bicyclo-[3.3.1]nonane ring system adopts a chair-boat conformation. In the crystal structure, the mol-ecules are linked by weak inter-molecular C-H⋯N hydro-gen bonds into chains along the b axis; additional stabilization is provide by C-H⋯π inter-actions.

No MeSH data available.


Related in: MedlinePlus