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(4-Chloro-benzohydrazidato-κN',O)[2-(4-chloro-benzoyl-hydrazono-κN,O)propionato(2-)-κO]oxidovanadium(V).

Wong HW, Lo KM, Ng SW - Acta Crystallogr Sect E Struct Rep Online (2009)

Bottom Line: In the crystal structure of the title compound, [VO(C(7)H(6)ClN(2)O)(C(10)H(7)ClN(2)O(3))], the V(V) atom is N,O-chelated by the chloro-benzoyl-hydrazidate anion and O,N,O'-chelated by the (chloro-benzoyl-hydrazono)propionate dianion.The distorted octa-hedral trans-N(2)O(4) coordination geometry is completed by the vanadyl O atom.In the crystal, mol-ecules are linked by N-H⋯O hydrogen bonds into a linear chain parallel to [010].

View Article: PubMed Central - HTML - PubMed

Affiliation: Department of Chemistry, University of Malaya, 50603 Kuala Lumpur, Malaysia.

ABSTRACT
In the crystal structure of the title compound, [VO(C(7)H(6)ClN(2)O)(C(10)H(7)ClN(2)O(3))], the V(V) atom is N,O-chelated by the chloro-benzoyl-hydrazidate anion and O,N,O'-chelated by the (chloro-benzoyl-hydrazono)propionate dianion. The distorted octa-hedral trans-N(2)O(4) coordination geometry is completed by the vanadyl O atom. In the crystal, mol-ecules are linked by N-H⋯O hydrogen bonds into a linear chain parallel to [010].

No MeSH data available.


Thermal ellipsoid plot (Barbour, 2001) of VO(C7H6ClN2O)(C10H7ClN2O3) at the 70% probability level. Hydrogen atoms are drawn as spheres of arbitrary radius.
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Fap1: Thermal ellipsoid plot (Barbour, 2001) of VO(C7H6ClN2O)(C10H7ClN2O3) at the 70% probability level. Hydrogen atoms are drawn as spheres of arbitrary radius.


(4-Chloro-benzohydrazidato-κN',O)[2-(4-chloro-benzoyl-hydrazono-κN,O)propionato(2-)-κO]oxidovanadium(V).

Wong HW, Lo KM, Ng SW - Acta Crystallogr Sect E Struct Rep Online (2009)

Thermal ellipsoid plot (Barbour, 2001) of VO(C7H6ClN2O)(C10H7ClN2O3) at the 70% probability level. Hydrogen atoms are drawn as spheres of arbitrary radius.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC2969368&req=5

Fap1: Thermal ellipsoid plot (Barbour, 2001) of VO(C7H6ClN2O)(C10H7ClN2O3) at the 70% probability level. Hydrogen atoms are drawn as spheres of arbitrary radius.
Bottom Line: In the crystal structure of the title compound, [VO(C(7)H(6)ClN(2)O)(C(10)H(7)ClN(2)O(3))], the V(V) atom is N,O-chelated by the chloro-benzoyl-hydrazidate anion and O,N,O'-chelated by the (chloro-benzoyl-hydrazono)propionate dianion.The distorted octa-hedral trans-N(2)O(4) coordination geometry is completed by the vanadyl O atom.In the crystal, mol-ecules are linked by N-H⋯O hydrogen bonds into a linear chain parallel to [010].

View Article: PubMed Central - HTML - PubMed

Affiliation: Department of Chemistry, University of Malaya, 50603 Kuala Lumpur, Malaysia.

ABSTRACT
In the crystal structure of the title compound, [VO(C(7)H(6)ClN(2)O)(C(10)H(7)ClN(2)O(3))], the V(V) atom is N,O-chelated by the chloro-benzoyl-hydrazidate anion and O,N,O'-chelated by the (chloro-benzoyl-hydrazono)propionate dianion. The distorted octa-hedral trans-N(2)O(4) coordination geometry is completed by the vanadyl O atom. In the crystal, mol-ecules are linked by N-H⋯O hydrogen bonds into a linear chain parallel to [010].

No MeSH data available.