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3-Bromo-N'-(3,5-dibromo-2-hydroxy-benzyl-idene)benzohydrazide methanol solvate.

Wei YJ, Wang FW, Zhu QY - Acta Crystallogr Sect E Struct Rep Online (2009)

Bottom Line: The dihedral angle between the two benzene rings is 5.5 (2)°.An intra-molecular O-H⋯N hydrogen bond is observed.In the crystal structure, pairs of adjacent Schiff base mol-ecules are linked by two methanol mol-ecules through inter-molecular N-H⋯O and O-H⋯O hydrogen bonds.

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Affiliation: Department of Chemistry, Huainan Normal College, Huainan 232001, People's Republic of China.

ABSTRACT
The title compound, C(14)H(9)Br(3)N(2)O(2)·CH(4)O, was prepared by the reaction of 3,5-dibromo-2-hydroxy-benzaldehyde and 3-bromo-benzohydrazide in methanol. The asymmetric unit of the crystal consists of a Schiff base mol-ecule and a methanol mol-ecule of crystallization. The dihedral angle between the two benzene rings is 5.5 (2)°. An intra-molecular O-H⋯N hydrogen bond is observed. In the crystal structure, pairs of adjacent Schiff base mol-ecules are linked by two methanol mol-ecules through inter-molecular N-H⋯O and O-H⋯O hydrogen bonds.

No MeSH data available.


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Molecular packing of the title compound. Hydrogen bonds are shown as dashed lines.
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Fap2: Molecular packing of the title compound. Hydrogen bonds are shown as dashed lines.


3-Bromo-N'-(3,5-dibromo-2-hydroxy-benzyl-idene)benzohydrazide methanol solvate.

Wei YJ, Wang FW, Zhu QY - Acta Crystallogr Sect E Struct Rep Online (2009)

Molecular packing of the title compound. Hydrogen bonds are shown as dashed lines.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC2968809&req=5

Fap2: Molecular packing of the title compound. Hydrogen bonds are shown as dashed lines.
Bottom Line: The dihedral angle between the two benzene rings is 5.5 (2)°.An intra-molecular O-H⋯N hydrogen bond is observed.In the crystal structure, pairs of adjacent Schiff base mol-ecules are linked by two methanol mol-ecules through inter-molecular N-H⋯O and O-H⋯O hydrogen bonds.

View Article: PubMed Central - HTML - PubMed

Affiliation: Department of Chemistry, Huainan Normal College, Huainan 232001, People's Republic of China.

ABSTRACT
The title compound, C(14)H(9)Br(3)N(2)O(2)·CH(4)O, was prepared by the reaction of 3,5-dibromo-2-hydroxy-benzaldehyde and 3-bromo-benzohydrazide in methanol. The asymmetric unit of the crystal consists of a Schiff base mol-ecule and a methanol mol-ecule of crystallization. The dihedral angle between the two benzene rings is 5.5 (2)°. An intra-molecular O-H⋯N hydrogen bond is observed. In the crystal structure, pairs of adjacent Schiff base mol-ecules are linked by two methanol mol-ecules through inter-molecular N-H⋯O and O-H⋯O hydrogen bonds.

No MeSH data available.


Related in: MedlinePlus