Limits...
Ethyl 4-hydroxy-methyl-2-methyl-pyridine-5-carboxyl-ate.

Boyd PD, Lena G, Spicer JA - Acta Crystallogr Sect E Struct Rep Online (2008)

Bottom Line: The title compound, C(10)H(13)NO(3), was obtained as a by-product of the aldolization reaction of furo[3,4-c]pyridin-3(1H)-one with thio-phene-2-carboxaldehyde.The substituents on the pyridine ring are nearly coplanar, with an 8.1 (2)° rotation of the hydroxmethyl group from this plane.The mol-ecules assemble in the crystal structure as chains via O-H⋯N hydrogen bonding between the pyridine N atom and a neighbouring hydroxy-methyl OH group.

View Article: PubMed Central - HTML - PubMed

ABSTRACT
The title compound, C(10)H(13)NO(3), was obtained as a by-product of the aldolization reaction of furo[3,4-c]pyridin-3(1H)-one with thio-phene-2-carboxaldehyde. The substituents on the pyridine ring are nearly coplanar, with an 8.1 (2)° rotation of the hydroxmethyl group from this plane. The mol-ecules assemble in the crystal structure as chains via O-H⋯N hydrogen bonding between the pyridine N atom and a neighbouring hydroxy-methyl OH group.

No MeSH data available.


Structure of (I) showing 50% probability displacement ellipsoids for non-hydrogen atoms and hydrogen atoms as arbitary spheres.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
getmorefigures.php?uid=PMC2961239&req=5

Fap1: Structure of (I) showing 50% probability displacement ellipsoids for non-hydrogen atoms and hydrogen atoms as arbitary spheres.


Ethyl 4-hydroxy-methyl-2-methyl-pyridine-5-carboxyl-ate.

Boyd PD, Lena G, Spicer JA - Acta Crystallogr Sect E Struct Rep Online (2008)

Structure of (I) showing 50% probability displacement ellipsoids for non-hydrogen atoms and hydrogen atoms as arbitary spheres.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC2961239&req=5

Fap1: Structure of (I) showing 50% probability displacement ellipsoids for non-hydrogen atoms and hydrogen atoms as arbitary spheres.
Bottom Line: The title compound, C(10)H(13)NO(3), was obtained as a by-product of the aldolization reaction of furo[3,4-c]pyridin-3(1H)-one with thio-phene-2-carboxaldehyde.The substituents on the pyridine ring are nearly coplanar, with an 8.1 (2)° rotation of the hydroxmethyl group from this plane.The mol-ecules assemble in the crystal structure as chains via O-H⋯N hydrogen bonding between the pyridine N atom and a neighbouring hydroxy-methyl OH group.

View Article: PubMed Central - HTML - PubMed

ABSTRACT
The title compound, C(10)H(13)NO(3), was obtained as a by-product of the aldolization reaction of furo[3,4-c]pyridin-3(1H)-one with thio-phene-2-carboxaldehyde. The substituents on the pyridine ring are nearly coplanar, with an 8.1 (2)° rotation of the hydroxmethyl group from this plane. The mol-ecules assemble in the crystal structure as chains via O-H⋯N hydrogen bonding between the pyridine N atom and a neighbouring hydroxy-methyl OH group.

No MeSH data available.