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3-(3-Chloro-prop-yl)-7,8-dimeth-oxy-2,3,4,5-tetra-hydro-1H-3-benzazepin-2-one at 125 K.

Cheng XW - Acta Crystallogr Sect E Struct Rep Online (2008)

Bottom Line: In the title compound, C(15)H(20)ClNO(3), the seven-membered ring adopts a distorted boat-sofa conformation; the methyl-ene C atoms of this ring are coplanar with the benzene ring.Both meth-oxy groups are almost coplanar with the attached benzene ring [C-C-O-C = 6.5 (2) and -13.5 (3)°].An intra-molecular C-H⋯O hydrogen bond is observed in the mol-ecular structure.

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Affiliation: Zhejiang Police College Experience Center, Zhejiang Police College, Hangzhou 310053, People's Republic of China.

ABSTRACT
In the title compound, C(15)H(20)ClNO(3), the seven-membered ring adopts a distorted boat-sofa conformation; the methyl-ene C atoms of this ring are coplanar with the benzene ring. Both meth-oxy groups are almost coplanar with the attached benzene ring [C-C-O-C = 6.5 (2) and -13.5 (3)°]. An intra-molecular C-H⋯O hydrogen bond is observed in the mol-ecular structure. In the crystal structure, a C-H⋯π inter-action involving the benzene ring is observed.

No MeSH data available.


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Crystal packing of the title compound, viewed approximately down the b axis. Dashed lines indicate intramolecular hydrogen bonds.
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Fap2: Crystal packing of the title compound, viewed approximately down the b axis. Dashed lines indicate intramolecular hydrogen bonds.


3-(3-Chloro-prop-yl)-7,8-dimeth-oxy-2,3,4,5-tetra-hydro-1H-3-benzazepin-2-one at 125 K.

Cheng XW - Acta Crystallogr Sect E Struct Rep Online (2008)

Crystal packing of the title compound, viewed approximately down the b axis. Dashed lines indicate intramolecular hydrogen bonds.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC2961196&req=5

Fap2: Crystal packing of the title compound, viewed approximately down the b axis. Dashed lines indicate intramolecular hydrogen bonds.
Bottom Line: In the title compound, C(15)H(20)ClNO(3), the seven-membered ring adopts a distorted boat-sofa conformation; the methyl-ene C atoms of this ring are coplanar with the benzene ring.Both meth-oxy groups are almost coplanar with the attached benzene ring [C-C-O-C = 6.5 (2) and -13.5 (3)°].An intra-molecular C-H⋯O hydrogen bond is observed in the mol-ecular structure.

View Article: PubMed Central - HTML - PubMed

Affiliation: Zhejiang Police College Experience Center, Zhejiang Police College, Hangzhou 310053, People's Republic of China.

ABSTRACT
In the title compound, C(15)H(20)ClNO(3), the seven-membered ring adopts a distorted boat-sofa conformation; the methyl-ene C atoms of this ring are coplanar with the benzene ring. Both meth-oxy groups are almost coplanar with the attached benzene ring [C-C-O-C = 6.5 (2) and -13.5 (3)°]. An intra-molecular C-H⋯O hydrogen bond is observed in the mol-ecular structure. In the crystal structure, a C-H⋯π inter-action involving the benzene ring is observed.

No MeSH data available.


Related in: MedlinePlus