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2-Anilino-3-benzoyl-4-(2,5-dichloro-phen-yl)-7,7-dimethyl-5-oxo-5,6,7,8-tetra-hydro-4H-benzo[b]pyran.

Wen LR, Sun JH, Ji C, Xie HY - Acta Crystallogr Sect E Struct Rep Online (2008)

Bottom Line: The title compound, C(30)H(25)Cl(2)NO(3), was prepared by the reaction of 3-oxo-N,3-diphenyl-propane-thio-amide, 2,5-dichloro-benzaldehyde and 5,5-dimethyl-1,3-cyclo-hexa-nedione (1:1:1) in ethanol.The cyclohexene ring adopts a half-chair conformation.The crystal structure exhibits intra-molecular N-H⋯O and C-H⋯O, and inter-molecular C-H⋯O inter-actions.

View Article: PubMed Central - HTML - PubMed

Affiliation: College of Chemistry and Molecular Engineering, Qingdao University of Science and Technology, Qingdao 266042, People's Republic of China.

ABSTRACT
The title compound, C(30)H(25)Cl(2)NO(3), was prepared by the reaction of 3-oxo-N,3-diphenyl-propane-thio-amide, 2,5-dichloro-benzaldehyde and 5,5-dimethyl-1,3-cyclo-hexa-nedione (1:1:1) in ethanol. The cyclohexene ring adopts a half-chair conformation. The crystal structure exhibits intra-molecular N-H⋯O and C-H⋯O, and inter-molecular C-H⋯O inter-actions.

No MeSH data available.


A packing diagram of (I), viewed down the a axis. The C—H···O interactions are shown as dashed lines.
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Fap2: A packing diagram of (I), viewed down the a axis. The C—H···O interactions are shown as dashed lines.


2-Anilino-3-benzoyl-4-(2,5-dichloro-phen-yl)-7,7-dimethyl-5-oxo-5,6,7,8-tetra-hydro-4H-benzo[b]pyran.

Wen LR, Sun JH, Ji C, Xie HY - Acta Crystallogr Sect E Struct Rep Online (2008)

A packing diagram of (I), viewed down the a axis. The C—H···O interactions are shown as dashed lines.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC2960223&req=5

Fap2: A packing diagram of (I), viewed down the a axis. The C—H···O interactions are shown as dashed lines.
Bottom Line: The title compound, C(30)H(25)Cl(2)NO(3), was prepared by the reaction of 3-oxo-N,3-diphenyl-propane-thio-amide, 2,5-dichloro-benzaldehyde and 5,5-dimethyl-1,3-cyclo-hexa-nedione (1:1:1) in ethanol.The cyclohexene ring adopts a half-chair conformation.The crystal structure exhibits intra-molecular N-H⋯O and C-H⋯O, and inter-molecular C-H⋯O inter-actions.

View Article: PubMed Central - HTML - PubMed

Affiliation: College of Chemistry and Molecular Engineering, Qingdao University of Science and Technology, Qingdao 266042, People's Republic of China.

ABSTRACT
The title compound, C(30)H(25)Cl(2)NO(3), was prepared by the reaction of 3-oxo-N,3-diphenyl-propane-thio-amide, 2,5-dichloro-benzaldehyde and 5,5-dimethyl-1,3-cyclo-hexa-nedione (1:1:1) in ethanol. The cyclohexene ring adopts a half-chair conformation. The crystal structure exhibits intra-molecular N-H⋯O and C-H⋯O, and inter-molecular C-H⋯O inter-actions.

No MeSH data available.