Limits...
N,N'-Bis(4-methyl-phen-yl)naphthalene-1,4-dicarboxamide N,N-dimethyl-acetamide disolvate.

Jing LH - Acta Crystallogr Sect E Struct Rep Online (2008)

Bottom Line: The two amide groups are approximately perpendicular to the naphthalene ring system [dihedral angles = 88.89 (1) and 89.08 (1)°].Each of the dimethyl-acetamide solvent mol-ecules are disordered over two positions, with occupancies of 0.655 (12):0.345 (12) and 0.531 (13):0.469 (13).The crystal packing is stabilized by N-H⋯O and C-H⋯O hydrogen bonds.

View Article: PubMed Central - HTML - PubMed

Affiliation: School of Chemistry and Chemical Engineering, China West Normal University, Nanchong 637002, People's Republic of China.

ABSTRACT
The title compound, C(26)H(22)N(2)O(2)·2C(4)H(9)NO, crystallizes in an anti C=O orientation. The two amide groups are approximately perpendicular to the naphthalene ring system [dihedral angles = 88.89 (1) and 89.08 (1)°]. Each of the dimethyl-acetamide solvent mol-ecules are disordered over two positions, with occupancies of 0.655 (12):0.345 (12) and 0.531 (13):0.469 (13). The crystal packing is stabilized by N-H⋯O and C-H⋯O hydrogen bonds.

No MeSH data available.


The asymmetric unit of the title compound. Displacement ellipsoids are drawn at the 30% probability level. All disordered components are shown. H atoms have been omitted for clarity.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
getmorefigures.php?uid=PMC2960113&req=5

Fap1: The asymmetric unit of the title compound. Displacement ellipsoids are drawn at the 30% probability level. All disordered components are shown. H atoms have been omitted for clarity.


N,N'-Bis(4-methyl-phen-yl)naphthalene-1,4-dicarboxamide N,N-dimethyl-acetamide disolvate.

Jing LH - Acta Crystallogr Sect E Struct Rep Online (2008)

The asymmetric unit of the title compound. Displacement ellipsoids are drawn at the 30% probability level. All disordered components are shown. H atoms have been omitted for clarity.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC2960113&req=5

Fap1: The asymmetric unit of the title compound. Displacement ellipsoids are drawn at the 30% probability level. All disordered components are shown. H atoms have been omitted for clarity.
Bottom Line: The two amide groups are approximately perpendicular to the naphthalene ring system [dihedral angles = 88.89 (1) and 89.08 (1)°].Each of the dimethyl-acetamide solvent mol-ecules are disordered over two positions, with occupancies of 0.655 (12):0.345 (12) and 0.531 (13):0.469 (13).The crystal packing is stabilized by N-H⋯O and C-H⋯O hydrogen bonds.

View Article: PubMed Central - HTML - PubMed

Affiliation: School of Chemistry and Chemical Engineering, China West Normal University, Nanchong 637002, People's Republic of China.

ABSTRACT
The title compound, C(26)H(22)N(2)O(2)·2C(4)H(9)NO, crystallizes in an anti C=O orientation. The two amide groups are approximately perpendicular to the naphthalene ring system [dihedral angles = 88.89 (1) and 89.08 (1)°]. Each of the dimethyl-acetamide solvent mol-ecules are disordered over two positions, with occupancies of 0.655 (12):0.345 (12) and 0.531 (13):0.469 (13). The crystal packing is stabilized by N-H⋯O and C-H⋯O hydrogen bonds.

No MeSH data available.