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N-(2,4-Dinitro-phen-yl)-N'-[nitro-(phenyl)-methyl-ene]hydrazine.

Yuan C - Acta Crystallogr Sect E Struct Rep Online (2008)

Bottom Line: The imine group is nearly coplanar with the (2,4-dinitro-phen-yl)-hydrazine unit.The second benzene ring and the third nitro group are twisted away from this plane, with dihedral angles of 48.5 (3) and 15.2 (3)°, respectively.Weak intra-molecular N-H⋯O inter-actions are observed.

View Article: PubMed Central - HTML - PubMed

Affiliation: Department of Chemistry and Chemical Engineering, Baoji College of Arts and Sciences, Baoji 721007, People's Republic of China.

ABSTRACT
The title compound, C(13)H(9)N(5)O(6), contains three nitro groups. It is prepared by the reaction of benzaldehyde 2,4-dinitro-phenyl-hydrazone with nitric oxide at ambient temperature. The imine group is nearly coplanar with the (2,4-dinitro-phen-yl)-hydrazine unit. The second benzene ring and the third nitro group are twisted away from this plane, with dihedral angles of 48.5 (3) and 15.2 (3)°, respectively. Weak intra-molecular N-H⋯O inter-actions are observed.

No MeSH data available.


The crystal packing of (I), viewed along the b axis.
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Fap2: The crystal packing of (I), viewed along the b axis.


N-(2,4-Dinitro-phen-yl)-N'-[nitro-(phenyl)-methyl-ene]hydrazine.

Yuan C - Acta Crystallogr Sect E Struct Rep Online (2008)

The crystal packing of (I), viewed along the b axis.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC2960026&req=5

Fap2: The crystal packing of (I), viewed along the b axis.
Bottom Line: The imine group is nearly coplanar with the (2,4-dinitro-phen-yl)-hydrazine unit.The second benzene ring and the third nitro group are twisted away from this plane, with dihedral angles of 48.5 (3) and 15.2 (3)°, respectively.Weak intra-molecular N-H⋯O inter-actions are observed.

View Article: PubMed Central - HTML - PubMed

Affiliation: Department of Chemistry and Chemical Engineering, Baoji College of Arts and Sciences, Baoji 721007, People's Republic of China.

ABSTRACT
The title compound, C(13)H(9)N(5)O(6), contains three nitro groups. It is prepared by the reaction of benzaldehyde 2,4-dinitro-phenyl-hydrazone with nitric oxide at ambient temperature. The imine group is nearly coplanar with the (2,4-dinitro-phen-yl)-hydrazine unit. The second benzene ring and the third nitro group are twisted away from this plane, with dihedral angles of 48.5 (3) and 15.2 (3)°, respectively. Weak intra-molecular N-H⋯O inter-actions are observed.

No MeSH data available.