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Ethyl 2-[(E)-4-(dimethyl-amino)benzyl-idenehydrazino]-5-nitro-benzoate.

Fun HK, Adhikari A, Patil PS, Kalluraya B, Chantrapromma S - Acta Crystallogr Sect E Struct Rep Online (2008)

Bottom Line: An intra-molecular N-H⋯O hydrogen bond involving the benzoate unit generates an S(6) ring motif.In the crystal, the mol-ecules are linked by weak C-H⋯O inter-actions into infinite chains along the b axis.These chains are further connected into sheets parallel to the ab plane which are stacked approximately along the c axis.

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ABSTRACT
The title compound, C(18)H(20)N(4)O(4), exists in the E configuration with respect to the C=N bond of the methyl-idine unit. The dihedral angle between the two benzene rings is 9.01 (6)°. An intra-molecular N-H⋯O hydrogen bond involving the benzoate unit generates an S(6) ring motif. In the crystal, the mol-ecules are linked by weak C-H⋯O inter-actions into infinite chains along the b axis. These chains are further connected into sheets parallel to the ab plane which are stacked approximately along the c axis. A C-H⋯π inter-action is also observed.

No MeSH data available.


Related in: MedlinePlus

The crystal packing of (I), viewed approximately along the c axis. Hydrogen bonds are drawn as dashed lines.
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Fap3: The crystal packing of (I), viewed approximately along the c axis. Hydrogen bonds are drawn as dashed lines.


Ethyl 2-[(E)-4-(dimethyl-amino)benzyl-idenehydrazino]-5-nitro-benzoate.

Fun HK, Adhikari A, Patil PS, Kalluraya B, Chantrapromma S - Acta Crystallogr Sect E Struct Rep Online (2008)

The crystal packing of (I), viewed approximately along the c axis. Hydrogen bonds are drawn as dashed lines.
© Copyright Policy - open-access
Related In: Results  -  Collection

License
Show All Figures
getmorefigures.php?uid=PMC2959927&req=5

Fap3: The crystal packing of (I), viewed approximately along the c axis. Hydrogen bonds are drawn as dashed lines.
Bottom Line: An intra-molecular N-H⋯O hydrogen bond involving the benzoate unit generates an S(6) ring motif.In the crystal, the mol-ecules are linked by weak C-H⋯O inter-actions into infinite chains along the b axis.These chains are further connected into sheets parallel to the ab plane which are stacked approximately along the c axis.

View Article: PubMed Central - HTML - PubMed

ABSTRACT
The title compound, C(18)H(20)N(4)O(4), exists in the E configuration with respect to the C=N bond of the methyl-idine unit. The dihedral angle between the two benzene rings is 9.01 (6)°. An intra-molecular N-H⋯O hydrogen bond involving the benzoate unit generates an S(6) ring motif. In the crystal, the mol-ecules are linked by weak C-H⋯O inter-actions into infinite chains along the b axis. These chains are further connected into sheets parallel to the ab plane which are stacked approximately along the c axis. A C-H⋯π inter-action is also observed.

No MeSH data available.


Related in: MedlinePlus